I need to measure levels of two inactive metabolites of
chloroacetaldehyde, 2- and 3- dechloroethylifosfamide, respectively.
The apparent method for measurement is to use a technique called
liquid-liquid extraction (LLE) using ethyle acetate, then resolving on
a Chirasil-L-val GC column and then detected via a
nitrogen-phosphorous-selective flame ionization detector. Does anyone
have any knowledge about this or know of a lab or company that could
run some plasma samples? Any help is greatly appreciated. Thanks in
advance.
Shayne Woodward
Surgical Research
Dartmouth College
Hanover, NH
