kzhao at biovx1.biology.ucla.edu wrote:
>> For Sunny's question of unprotection of glucuronide:
>> Dissolve your compound in methanol (cold), flux ammonia for 1hr during stirring,
> and store in a refrigerator o/n. Acetate is recovered by filtration. See
> J. Histochem. Cytochem. 2: 209-229, 1954 for details on similar compound.
>> Good luck,
>> Ke-Wei Zhao, Ph.D.
> Dept. Biol. Chem.
> UCLA School of Medicine
> Los Angeles, CA 90095
++++++++++++++++++++++++++++++++
Any chance of ending up with glucuronamide under the stated conditions?
Might KCN/MeOH do better? Mind you, careful of HCN vapors on work-up!
Juan
